Very low temperature NMR method and device
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United States of America Patent
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Jun 12, 2018
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app pub date -
Dec 11, 2012
filing date -
Dec 13, 2011
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Abstract
The NMR analysis method for analyzing a solid sample positioned in a sample-holder (21) includes generation of a plurality of high-pressure gaseous flows (2, 3, 4) from at least one first source (1) of a high-pressure gas; cooling of the gaseous flows (2, 3, 4) in at least one heat exchanger (12) from a coolant gas (15) originating from at least one second source (11) of gas; and rotation of the sample-holder (21) by a first cooled high-pressure gaseous flow (2) and cooling of the sample-holder by a second cooled high-pressure gaseous flow (3).
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