Temperature modulated thermogravimetric analysis
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United States of America Patent
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Nov 14, 2017
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app pub date -
May 6, 2015
filing date -
May 6, 2014
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Abstract
A sample is analyzed by temperature-modulated thermogravimetric analysis (TMTGA), using a thermogravimetric analysis (TGA) instrument. The TGA instrument comprises a furnace arranged in a furnace housing and an electronic balance with a load receiver arranged in a balance housing, wherein the load receiver extends into the furnace housing. A measuring position is arranged at one end of the load receiver within the furnace housing. A control unit controls the balance and/or the furnace. The TMTGA method includes at least using the TGA instrument to subject the sample to a temperature program that varies the temperature of the furnace and provides temperature-time setpoints for controlling the sample temperature, measuring the mass change of the sample as a function of time, and determining at least one kinetic parameter of the sample based on mass change. The temperature program may be stochastic and/or event-controlled in nature.
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