Processes for producing acetic acid with decanter control

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United States of America Patent

PATENT NO 9695101
APP PUB NO 20160137581A1
SERIAL NO

14873614

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Abstract

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A process for producing acetic acid comprising the steps of carbonylating methanol in a reaction medium to form a crude acetic acid product; conveying the crude acetic acid product to a flash vessel at a flash flow rate; flashing the crude acetic acid product to form a first vapor stream comprising acetic acid and a liquid residue stream comprising metal catalyst and halide salt; separating the flashed vapor stream to form a second vapor stream comprising methyl iodide a sidedraw comprising purified acetic acid and water, and a liquid residue stream. The process further comprises the steps of condensing at least a portion of the second vapor stream to form at least one liquid phase and refluxing to the light ends column at least a portion of the at least one liquid phase at a reflux rate. The reflux rate is adjusted based on changes in the flash flow rate.

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Patent Owner(s)

Patent OwnerAddress
CELANESE INTERNATIONAL CORPORATION222 W LAS COLINAS BLVD SUITE 900N IRVING TX 75039

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Liu, Yaw-Hwa Missouri City, US 38 82
Scates, Mark O Houston, US 114 1958
Shaver, Ronald D Houston, US 49 100

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