Reactive chromatography process for equilibrium-limited reactions
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United States of America Patent
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Apr 25, 2017
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May 2, 2014
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May 3, 2013
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Abstract
The present disclosure provides for a process for an equilibrium limited reaction using reactive chromatography unit (RCU) in which a first organic donor reactant (FODR) and a second organic acceptor reactant (SOAR) react to form a product mixture of a first acceptor product (FAP) and a second donor co-product (SDCP). The equilibrium-limited reaction does not produce water. The RCU has separation media to separate the product mixture into a raffinate and an extract. The FODR is in a stoichiometric deficit relative to the SOAR for the equilibrium limited reaction, so that the SOAR acts as the eluent for both the raffinate and the extract, and so as not to produce an azeotrope of FODR and the SDCP in the extract.
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