Method for preparation of an alane-etherate complex and alane
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United States of America Patent
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Jan 24, 2017
Grant Date -
Apr 2, 2015
app pub date -
Dec 2, 2014
filing date -
Jun 5, 2012
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Abstract
The invention relates to methods of forming an alane-etherate complex and α-alane from the alane-etherate complex. The methods include reacting an alkyl halide with a metal alanate in a solvent including an ether. A tertiary amine may also be added to the reaction. The alane is collected after removal of the solvent and/or the tertiary amine. An electrospraying process can be used to remove the solvent.
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