Apparatus and method for solid phase synthesis
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United States of America Patent
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Jan 3, 2017
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Aug 13, 2015
app pub date -
Sep 2, 2013
filing date -
Aug 31, 2012
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Abstract
An apparatus for microwave assisted solid phase synthesis using solid-phase resin beads mixed with a liquid solvent comprising a generally cylindrical reactor made of microwave transparent material and having a central axis, the reactor having an inlet and an outlet; a porous frit associated with the outlet of the reactor, the porous frit preventing discharge of beads and allowing discharge of the solvent from the reactor; and means for concentric rotation of the reactor around the central axis in alternating clockwise and anti-clockwise directions. A method for microwave assisted solid phase synthesis using the apparatus is also disclosed.
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