Process for isolation of fatty acids, resin acids and sterols from tall oil pitch

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United States of America Patent

PATENT NO 9422507
APP PUB NO 20130261284A1
SERIAL NO

13875050

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Abstract

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A process for recovering fatty acids, resin acids and sterols from tall oil pitch, said process comprising

    a) saponifying the tall oil pitch with an alkali to hydrolyze esters included in the pitch to free alcohols and organic acids in salt form,b) acidulating the saponified pitch with a mineral acid to convert the organic acids in salt form into free organic acids and to form an organic phase and an aqueous phase,c) separating the aqueous phase from the organic phase,d) evaporation fractionating the organic phase to obtain a distillate rich in sterols, fatty acids and resin acids,d) evaporation fractionating the organic phase to obtain a distillate rich in sterols, fatty acids and resin acids,e) evaporation fractionating the distillate to obtain a bottom fraction rich in sterols, and a distillate rich in fatty acids and resin acids, andf) subjecting the sterols in the sterol-rich bottom fraction to crystallization purification.

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Patent Owner(s)

Patent OwnerAddress
RAVINTORAISIO OY21200 RAISIO

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Hamunen, Antti Turku, FI 12 41

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