Method for synthesizing rare earth metal extractant

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United States of America Patent

PATENT NO 9133100
APP PUB NO 20130123534A1
SERIAL NO

13808220

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Abstract

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A rare earth metal extractant containing, as the extractant component, dialkyldiglycol amide acid which is excellent in breaking down light rare earth elements is reacted in diglycolic acid (X mol) and an esterification agent (Y mol) at a reaction temperature of 70° C. or more and for a reaction time of one hour or more such that the mol ratio of Y/X is 2.5 or more, and is subjected to vacuum concentration. Subsequently, a reaction intermediate product is obtained by removing unreacted products and reaction residue. Then a nonpolar or low-polar solvent which is an organic solvent for forming an organic phase during solvent extraction of the rare earth metal and which is capable of dissolving dialkyldiglycol amide acid is added as the reaction solvent, and the reaction intermediate product is reacted with dialkyl amine (Z mol) such that the mol ratio of Z/X is 0.9 or more.

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Patent Owner(s)

Patent OwnerAddress
SHIN-ETSU CHEMICAL CO LTDTOKYO 1000005
JAPAN ATOMIC ENERGY AGENCYIBARAKI 319-1184

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Kume, Tetsuya Echizen, JP 29 89
Naganawa, Hirochika Naka-gun, JP 13 63
Ohashi, Masaki Joetsu, JP 190 2040
Sakaki, Kazuaki Echizen, JP 20 129
Shimojo, Kojiro Naka-gun, JP 6 49
Sugahara, Hiroto Echizen, JP 340 2566

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