Method for completely dissolving and rapidly hydrolyzing cellulose, and uses of said method
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United States of America Patent
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Aug 25, 2015
Grant Date -
Mar 22, 2012
app pub date -
Aug 18, 2010
filing date -
Feb 2, 2010
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Abstract
The invention discloses a method for completely dissolving and rapidly hydrolyzing cellulose, and uses thereof. Cellulose is placed in an acidic aqueous solution with a [H+] concentration of 10−7˜1 M or an alkaline aqueous solution with a [OH−] concentration of 10−7˜1 M as sample A, wherein the volume ratio of solid to liquid is (0.003˜1.05):1. The acidic aqueous solution with a [H+] concentration of 10−7˜1 M or the alkaline aqueous solution with a [OH−] concentration of 10−7˜1 M is heated up to 261˜352 as sample B. Sample A and sample B obtained from step 1 and step 2 are mixed in a reactor to a concentration of cellulose of 0.1%˜35%, the concentration of the mixed solution is adjusted to an acidity of 10−7˜1 M [H+] or an alkalinity of 10−7˜1 M [OH−], and a water density of 587˜997 kg/m3, pressure is set at 6˜584 MPa. The mixture is rapidly heated up to 261˜352 at heating rate of 7.8˜14.8 /s, and then cellulose is dissolved completely in 0.8˜2 sec and hydrolyzed in 5 sec. Using this technique, it is the first time for achieving complete dissolution and rapid hydrolysis of cellulose at a lower temperature, which not only dramatically reduces the cost of hydrolysis but also improves the safety of production and extends the service life of equipment, thus possessing a good application prospect.

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- 15 United States
- 10 France
- 8 Japan
- 7 China
- 5 Korea
- 2 Other
Patent Owner(s)
Patent Owner | Address | |
---|---|---|
XISHUANGBANNA TROPICAL BOTANICAL GARDEN CHINESE ACADEMY OF SCIENCES | YUNNAN PROVINCE KUNMING CITY XUEFU ROAD 650223 NO 50 XISHUANGBANNA TROPICAL BOTANICAL GARDEN KUNMING BRANCH KUNMING CITY YUNNAN PROVINCE 650223 |
International Classification(s)

- [Classification Symbol]
- [Patents Count]
Inventor(s)
Inventor Name | Address | # of filed Patents | Total Citations |
---|---|---|---|
Fang, Zhen | Kunming, CH | 51 | 485 |
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11.5 Year Payment | $7400.00 | $3700.00 | $1850.00 | Feb 25, 2027 |
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Surcharge - 11.5 year - Late payment within 6 months | $160.00 | $80.00 | $40.00 |
Surcharge after expiration - Late payment is unavoidable | $700.00 | $350.00 | $175.00 |
Surcharge after expiration - Late payment is unintentional | $1,640.00 | $820.00 | $410.00 |
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