Method for extracting vanadium from shale
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United States of America Patent
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Feb 3, 2015
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app pub date -
Aug 26, 2013
filing date -
Nov 14, 2012
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Abstract
A method for extracting vanadium from shale, the method including: a) grinding the shale into fine powders, mixing the fine powders with an additive in a mass ratio of 1:0.04-0.12 to yield a mixture, heating the mixture to a temperature of between 850 and 950° C. at a heating rate of 5-9° C./min, and baking the mixture for between 30 and 90 min; b) immersing the product in water and acid respectively to yield a first solution and a second solution, combining the two solutions, and performing ion exchange adsorption on the combined solution using a styrene-divinylbenzene based macroporous anion-exchange resin; and c) performing desorption, purification, and precipitation to yield poly ammonium vanadate, and calcining the poly ammonium vanadate at a temperature of between 450 and 530° C. for between 20 and 50 min to yield V2O5.
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