Method of producing alkoxysilanes and precipitated silicas from biogenic silicas
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United States of America Patent
Stats
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Dec 23, 2014
Issued Date -
N/A
app pub date -
Jan 9, 2013
filing date -
Jan 17, 2012
priority date (Note) -
In Force
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Abstract
A method of producing alkoxysilanes and precipitated silicas from biogenic silicas is provided. In a first step, biogenically concentrated silica is mixed with a liquid polyol to obtain a mixture, and then the mixture is heated. In a second step, a base is added to obtain a reaction mixture. In a third step, the reaction mixture is filtered to remove the carbon enriched RHA or other undissolved biogenic silica and recover the solution of alkoxysilane and alcoholate. In a fourth step, alkoxysilane is purified by filtering, distilling, precipitating or extracting from the original reaction solution to precipitate various forms of silica. In a final step, residual base present in alkoxysilane is neutralized to eliminate the residual alkali metal base.
First Claim
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Family

- 15 United States
- 10 France
- 8 Japan
- 7 China
- 5 Korea
- 2 Other
Patent Owner(s)
Patent Owner | Address | |
---|---|---|
LAINE RICHARD M | 1375 FOLKSTONE CT ANN ARBOR MI 48105 |
International Classification(s)

- 2013 Application Filing Year
- C01B Class
- 1318 Applications Filed
- 1164 Patents Issued To-Date
- 88.32 % Issued To-Date
Inventor(s)
Inventor Name | Address | # of filed Patents | Total Citations |
---|---|---|---|
Krug, David J | Ann Arbor, US | 13 | 46 |
# of filed Patents : 13 Total Citations : 46 | |||
Laine, Richard M | Ann Arbor, US | 54 | 1106 |
# of filed Patents : 54 Total Citations : 1106 | |||
Marchal, Julien C | Ann Arbor, US | 4 | 8 |
# of filed Patents : 4 Total Citations : 8 | |||
Popova, Vera | Ann Arbor, US | 5 | 18 |
# of filed Patents : 5 Total Citations : 18 |
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Patent Citation Ranking
- 3 Citation Count
- C01B Class
- 13.95 % this patent is cited more than
- 11 Age
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11.5 Year Payment | $7400.00 | $3700.00 | $1850.00 | Jun 23, 2026 |
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Surcharge after expiration - Late payment is unavoidable | $700.00 | $350.00 | $175.00 |
Surcharge after expiration - Late payment is unintentional | $1,640.00 | $820.00 | $410.00 |
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Mar 04, 2022 | MAFP | MAINTENANCE FEE PAYMENT | free format text: PAYMENT OF MAINTENANCE FEE, 8TH YR, SMALL ENTITY (ORIGINAL EVENT CODE: M2552); ENTITY STATUS OF PATENT OWNER: SMALL ENTITY year of fee payment: 8 |
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Dec 21, 2017 | AS | ASSIGNMENT | free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNOR:MAYATERIALS, INC.;REEL/FRAME:044968/0879 Owner name: LAINE, RICHARD M, MICHIGAN Effective Date: Dec 21, 2017 |
Dec 23, 2014 | I | Issuance | |
Dec 03, 2014 | STCF | INFORMATION ON STATUS: PATENT GRANT | free format text: PATENTED CASE |
Jul 18, 2013 | P | Published | |
Jan 09, 2013 | F | Filing | |
Jan 09, 2013 | AS | ASSIGNMENT | free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNORS:LAINE, RICHARD M;MARCHAL, JULIEN C;POPOVA, VERA;AND OTHERS;SIGNING DATES FROM 20130102 TO 20130108;REEL/FRAME:029593/0950 Owner name: MAYATERIALS INC., MICHIGAN |
Jan 17, 2012 | PD | Priority Date |

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