Process for continuous preparation of a prepolymer based on phenolic resins, oxazolines and epoxides

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United States of America Patent

PATENT NO 8834971
APP PUB NO 20120121812A1
SERIAL NO

13297906

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Abstract

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Process for the continuous preparation of prepolymers based on phenolic resin, an oxazoline component and an epoxide in the presence of a catalyst, including supplying the phenolic resin and the oxazoline component to an extruder in a stream A; a Lewis adduct of boron trifluoride or of aluminum trichloride, or arylsulphonic acids or alkylsulphonic acids, or latent arylsulphonic acids or latent alkylsulphonic acids, in a stream B, and the epoxide in a stream C, the infeed of stream A being situated, as seen in extrusion direction, before the infeed of stream C, these reactants are mixed at a reaction temperature of 120 to 200° C. with a residence time in the extruder of 3 seconds to 15 minutes, and then the product discharge of the extruder is cooled to a temperature of less than 45° C. within from 30 to 60 seconds.

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Patent Owner(s)

Patent OwnerAddress
EVONIK OPERATIONS GMBHRELLINGHAUSER STRASSE 1-11 ESSEN 45128

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Omeis, Marianne Dorsten, DE 13 59
von, Itter Franz-Albert Alfter, DE 4 13
Weihrauch, Thomas Duelmen, DE 18 65

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