Method of preparing metal nitride and/or metal oxynitride particulate material as nanoparticles, microparticles, nanotubes, bulk powder, and/or coatings from organometallic precursors, and precursors therefor
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United States of America Patent
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Jul 29, 2014
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app pub date -
Feb 5, 2009
filing date -
Feb 5, 2008
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Abstract
A method of preparing a metal nitride and/or metal oxynitride particulate material includes heating a stoichiometric mixture of a metal compound and urea at a temperature of about 400-1000° C. for a predetermined time period in the presence of argon, nitrogen, or both. The particulate material produced includes nanoparticles, nanotubes, microparticles, powder, or a combination thereof.
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