Preparation method of MLN4924 as an E1 activating inhibitor
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United States of America Patent
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May 6, 2014
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Mar 20, 2012
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Jun 22, 2011
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Abstract
The present invention relates to a method for preparation of MLN4924 as an E1 activating inhibitor, and more specifically, to a method for efficient and stereoselective preparation of MLN4924 by means of key steps involving stereoselective reduction of cyclopentenone with isopropylidene, regioselective cleavage of isopropylidene moiety, and synthesis of cyclic sulfate.
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