Methods of preparing clusterboron
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United States of America Patent
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Jan 7, 2014
Grant Date -
Aug 11, 2011
app pub date -
Nov 3, 2008
filing date -
Nov 2, 2007
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Abstract
The invention provides new methods for synthesis of ClusterBoron (B18H22). Preferred methods of the invention include in situ generation of the conjugate acid of B20H182− and degradation of the acid in solution to produce B18H22 in high yields and high purity. The invention further provides isotopically enriched boranes, particularly isotopically enriched 10B)18H22 and 11B18H22.
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