Process for the production of a titanium silicalite shaped article
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United States of America Patent
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May 28, 2013
Grant Date -
Jul 10, 2003
app pub date -
Mar 21, 2001
filing date -
Mar 29, 2000
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Abstract
A process for the production of a titanium silicalite shaped article by: a) preparation of a synthesis gel containing a Si2 source, a Ti2 source, a template compound and water, b) crystallization of the synthesis gel under hydrothermal conditions, c) drying of the titanium silicalite from step b) at a temperature below the decomposition temperature of the template compound, d) preparation of a formable mass containing the product from step c), a binder and a paste-forming agent, e) forming of the mass from step d) into a green shaped article, f) optionally drying, and g) calcinations of the green shaped article, as well as a titanium silicalite shaped article obtainable according to this process, and the use of this shaped article as a catalyst in epoxidation or ammoximation reactions.
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