Freeze-drying method and freeze-drying apparatus

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United States of America Patent

PATENT NO 8365432
APP PUB NO 20110016741A1
SERIAL NO

12933225

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Abstract

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A material to be dried is frozen and is efficiently freeze-dried in a short time, thereby increasing production efficiency. A freeze-drying apparatus includes a vertical tube (2) having an inner circumferential surface formed with a frozen surface (2a), a liquid-supply device (5) for supplying a liquid material to be dried (47) onto the frozen surface (2a), a freezing device (10) arranged around the vertical tube (2) and intended for cooling the frozen surface (2a), a pressure-reduction device (12) which puts an interior area of the vertical tube (2) into a state of vacuum, and an internal heating device (41) in the vertical tube (2). The internal heating device (41) is arranged in the vertical tube (2) along a center axis thereof, and has an outer surface formed with a vertically long circular-cylindrical radiation surface (43). The liquid material to be dried (47) supplied from the liquid-supply device (5) is sprinkled onto the frozen surface (2a), and the frozen surface (2a) is cooled to freeze the dried material (47) into a shape of a pipe. Then, the interior area of the vertical tube (2) is pressure-reduced to supply radiation heat from the internal heating device (41) to the dried material (47) for freeze-drying the dried material (47).

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Patent Owner(s)

Patent OwnerAddress
MORIMOTO-PHARMA CO LTDNISHIYODOGAWA-KU OSAKA-SHI OSAKA 555-0012
UNITEC CO LTD1-60 TSUNEYOSHI 1-CHOME KONOHANA-KU OSAKA-SHI OSAKA 554-0052
PHARMA-TECH CO LTD41-4-210 YAMADAHIGASHI 4-CHOME SUITA-SHI OSAKA 565-0821

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Morimoto, Shuji Suita, JP 27 940

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