Acid resistant particles of an alkaline earth metal carbonate
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United States of America Patent
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Dec 4, 2012
Grant Date -
Feb 18, 2010
app pub date -
Dec 20, 2005
filing date -
Dec 22, 2004
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Abstract
Alkaline earth metal carbonate exhibiting a resistance to acids expressed as pH of less than 7 measured after suspending 1.0 g of the particles in a mixture made of 20 ml of toluene and 80 ml of an aqueous phase consisting of deionized water, 11.76 g/L of citric acid monohydrate, 2.57 g/L of NaCl and 0.068 mol/L of NaOH, after 35 minutes of stirring at 25° C. and at 1 000 rpm, or expressed as a moisture pick-up lower than or equal to 2 g water/kg of calcium carbonate after one week of storage at 22° C. and 50% relative humidity, or as a Differential Scanning Calorimetry (DSC) spectrum showing at least one peak between 170 and 190° C. when measured at a heating rate of 10° C./min under nitrogen atmosphere from 25 to 250° C. in open cells. Process for the preparation of said particles, compositions containing said particles and the use thereof.
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