C methyl iodide
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United States of America Patent
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May 29, 2012
Grant Date -
Aug 28, 2008
app pub date -
Mar 23, 2006
filing date -
Mar 23, 2005
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Expired
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Abstract
A process for the preparation of 11C methyl iodide comprises coating the internal surface of a first reaction vessel with a solution of lithium aluminum hydride, wherein the first reaction vessel has an internal diameter not greater than about 1.5 mm; introducing 11C carbon dioxide into the first reaction vessel such that it is reduced by the lithium aluminum hydride to give a reduction product; and reacting the reduction product with hydriodic acid.
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