Method for adiabatic cooling type crystallization of organic compound and apparatus therefor
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United States of America Patent
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Apr 24, 2012
Grant Date -
Apr 30, 2009
app pub date -
Mar 7, 2006
filing date -
Mar 30, 2005
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Abstract
A method including carrying out adiabatic cooling and evaporation operation of a coolant in a crystallizer (20) for a mixture solution of a target organic compound containing the coolant; taking out crystal slurry produced by the operation from the crystallizer (20); pressurizing evaporated vapor to a pressure higher than the operation pressure in the crystallizer (20) by a compressor (30) and then introducing the vapor to an absorption condenser (10); cooling for condensation the mixture solution of organic compound and the evaporated vapor that has been pressurized while allowing them to contact each other in the absorption condenser (10); introducing the crystal slurry taken out of the crystallizer (20) to a purification means (70) for purification of the crystal; and introducing a clarified liquid in the purification means (70) to at least one of the crystallizer (20) and the absorption condenser (10).
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