Method of synthesizing small-diameter carbon nanotubes with electron field emission properties

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United States of America Patent

PATENT NO 7618300
APP PUB NO 20060055303A1
SERIAL NO

11012341

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Abstract

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Carbon nanotube material having an outer diameter less than 10 nm and a number of walls less than ten are disclosed. Also disclosed are an electron field emission device including a substrate, an optionally layer of adhesion-promoting layer, and a layer of electron field emission material. The electron field emission material includes a carbon nanotube having a number of concentric graphene shells per tube of from two to ten, an outer diameter from 2 to 8 nm, and a nanotube length greater than 0.1 microns. One method to fabricate carbon nanotubes includes the steps of (a) producing a catalyst containing Fe and Mo supported on MgO powder, (b) using a mixture of hydrogen and carbon containing gas as precursors, and (c) heating the catalyst to a temperature above 950° C. to produce a carbon nanotube. Another method of fabricating an electron field emission cathode includes the steps of (a) synthesizing electron field emission materials containing carbon nanotubes with a number of concentric graphene shells per tube from two to ten, an outer diameter of from 2 to 8 nm, and a length greater than 0.1 microns, (b) dispersing the electron field emission material in a suitable solvent, (c) depositing the electron field emission materials onto a substrate, and (d) annealing the substrate.

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Patent Owner(s)

Patent OwnerAddress
NURAY TECHNOLOGY CO LTDMIDDLE HUACHENG ROAD ROOM 216 NO 168 JINTAN JIANGSU PROVINCE 213200

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Du, Chunsheng Davis , US 9 148
Gao, Bo Elon , US 577 2816
Liu, Jie Chapel Hill , US 812 14130
Qian, Cheng Durham , US 88 384
Qiu, Qi Cary , US 21 459
Zhou, Otto Z Chapel Hill , US 55 2576

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