Process for producing monopentaerythritol of high purity and monopentaerythritol produced by the process

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United States of America Patent

PATENT NO 7569736
APP PUB NO 20090062575A1
SERIAL NO

12162423

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ATTORNEY / AGENT: (SPONSORED)

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Abstract

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The invention relates to a process for producing monopentaerythritol of high purity and monopentaerythritol produced by the process. Formaldehyde is reacted with acetaldehyde in an aqueous solution in the presence of a strongly basic hydroxide in a conventional way. The obtained reaction mixture is evaporated to a dryness of 50-70% by weight and is thereafter cooled. Crystals of pentaerythritol thereby formed are separated off. The crystals are dissolved in water or in a water-containing mother liquor containing pentaerythritol to a dryness of 35-55% by weight. The solution is treated in a purification step whereupon monopentaerythritol of high purity is crystallized at a temperature of 40-90° C. and separated from the remaining mother liquor which is recirculated to the above mentioned step.

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Patent Owner(s)

Patent OwnerAddress
PERSTORP SPECIALTY CHEMICALS AB284 80 PERSTORP

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Bengtsson, Hans-Ake Bjarnum , SE 1 2
Nyman, Lars-Henrik Hassleholm , SE 1 2

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