Method for the manufacture of caprolactam from waste containing polyamides
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United States of America Patent
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Feb 6, 2007
Grant Date -
Feb 5, 2004
app pub date -
Jun 9, 2003
filing date -
Jun 10, 2002
priority date (Note) -
Expired
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Abstract
This invention relates to a continuous and efficient method for the manufacture of highly pure caprolactam suitable for the polycondensation of Polyamide 6 (polycaprolactam) from polyamide waste. In particular the invention relates to a method for the manufacture of caprolactam from waste containing polyamides, including the steps a) depolymerisation of the waste containing polyamides, whereby a caprolactam raw material and a flow containing secondary constituents or additives is obtained, b) at least one distillation of the caprolactam raw material, and c) at least one crystallisation of the caprolactam material obtained in step b), by which means caprolactam is obtained, whereby at least part of the caprolactam obtained in step c) with a permanganate number of<10000 sec. and a UV transmission of<85% is added to the waste containing polyamides before and/or during the depolymerisation.
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