Method for producing polysulfides by means of electrolytic oxidation
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United States of America Patent
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Feb 11, 2003
Grant Date -
May 9, 2002
app pub date -
Aug 27, 2001
filing date -
Feb 26, 1999
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Abstract
The present invention has an object to obtain a cooking liquor containing polysulfide-sulfur at a high concentration by minimizing by-production of thiosulfate ions. The present invention is a method for producing polysulfides, which comprises introducing a solution containing sulfide ions into an anode compartment of an electrolytic cell comprising the anode compartment provided with a porous anode, a cathode compartment provided with a cathode, and a diaphragm partitioning the anode compartment and the cathode compartment, for electrolytic oxidation to obtain polysulfide ions, characterized in that the porous anode is disposed so that a space is provided at least partly between the porous anode and the diaphragm, and the apparent volume of the porous anode is from 60% to 99% based on the volume of the anode compartment.
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