Process for the preparation of phosphonite compounds

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United States of America Patent

PATENT NO 6437164
SERIAL NO

09869865

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Abstract

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Biphenyl and phosphorus trichloride are reacted in the presence of aluminum chloride, a hydrogen chloride gas generated is removed, a pyridine is added, excess phosphorus trichloride is removed, a resulting reaction product containing the obtained phosphine compound of the formula: ##STR1## and a phenol compound of the formula: ##STR2## wherein R is a hydrogen atom or methyl and R.sup.1 and R.sup.2 are each a hydrogen atom or alkyl having 1 to 5 carbon atoms, are reacted in the presence of a base as a deacidifying agent, and hydrochloride of this base and a pyridine-aluminum chloride complex are removed. By this method, a high quality phosphonite compound containing phosphinobiphenylene of the formula: ##STR3## can be produced safely in a high yield.

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Patent Owner(s)

Patent OwnerAddress
API CORPORATION13-4 UCHIKANDA 1-CHOME CHIYODA-KU TOKYO 1010047

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Kasagi, Masahiro Fukuoka, JP 1 2
Mishima, Akio Fukuoka, JP 31 242
Ozaki, Yoshihiro Osaka, JP 32 172
Yamamoto, Masataka Fukuoka, JP 64 635
Yokomatsu, Takashi Mie, JP 1 2

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