Processes for producing citrate esters

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United States of America Patent

PATENT NO 6403825
SERIAL NO

09437334

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Abstract

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Described are processes for producing citrate esters in, an economic fashion. Esters are prepared by esterification of a citric acid-containing fermentation broth having been treated to remove cations and optionally other impurities, but containing sugar(s). Esters are also prepared by reacting an impure aqueous citric acid source with an alcohol to provide a heterogeneous aqueous/organic reacted mixture, wherein the organic phase contains the ester and the aqueous phase retains water-soluble impurities. A liquid phase separation is then used to separate the organic and aqueous phases, conveniently separating the impurities from the product and avoiding the energy-intensive distillation of water from the reaction medium.

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Patent OwnerAddress
WILMINGTON TRUST NATIONAL ASSOCIATION AS COLLATERAL AGENT50 SOUTH SIXTH STREET SUITE 1290 MINNEAPOLIS MN 55402

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Chiu, Kuen-Wai Greensboro, NC 6 21
Davis, James E Greensboro, NC 70 1738
Frappier, Edward P Kernersville, NC 12 115
Grendze, Martin Indianapolis, IN 9 20
Scriven, Eric F V Greenwood, IN 25 72
Wyeth, John T Indianapolis, IN 3 17

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