Preparation of di-t-alkyl peroxides and t-alkyl hydroperoxides from n-alkyl ethers
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United States of America Patent
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May 1, 2001
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N/A
app pub date -
Dec 10, 1999
filing date -
Dec 10, 1999
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Abstract
A process for production of a t-alkyl peroxide compound includes the steps of: a) reacting an n-alkyl t-alkyl ether with a reactant mixture comprising an acid catalyst and a compound of the formula RO.sub.2 H (I) where R is H or t-alkyl, provided that if R is t-alkyl the t-alkyl peroxide compound product is a di-t-alkyl peroxide, and b) isolating a reaction product comprising said t-alkyl peroxide compound from the mixture resulting from step a). The process can be used to prepare t-butyl hydroperoxide or di-t-butyl peroxide from methyl t-butyl ether. Sulfuric acid may be used as the acid catalyst.
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