Process for the production of 2,5-dimethyl-2,5-di-t-butylperoxy-hexane
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United States of America Patent
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Mar 7, 2000
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N/A
app pub date -
Oct 12, 1998
filing date -
Apr 17, 1996
priority date (Note) -
Expired
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Abstract
2,5-dimethyl-2,5-di-t-butylperoxy-hexane is produced by reacting 2,5-dimethyl-1,5-hexadiene with t-butylhydroperoxide under acid catalysis in the presence of an electron pair acceptor Lewis acid in a substantially anhydrous solvent. If one uses technical water-containing t-butylhydroperoxide, the water can be separated, after mixing with the 2,5-dimethyl-1,5-hexadiene, by adding sulfuric acid or calcium chloride and subsequently the electron pair acceptor Lewis acid is added.
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