Aqueous method to prepare cyclopropyl methylketone from acetyl-propanol

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United States of America Patent

PATENT NO 6025528
SERIAL NO

09033762

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Abstract

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An entirely aqueous method to prepare cyclopropyl methylketone from acetyl-propanol. The method is practiced by (1) forming a mixture of acetyl-propanol and an aqueous hydrogen halide, (2) distilling the mixture and returning at least a portion of the distillate that is aqueous to the distilland, (3) recovering 5-halo-2-pentanone from the distillate, and (4) reacting the 5-halo-2-pentanone with a basic solution that is from about 1-wt % to about 25-wt % base and about 75-wt % to about 99-wt % water to yield cyclopropyl methylketone.

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PCBU SERVICES INC9TH FLOOR-DE5403 300 DELAWARE AVENUE WILMINGTON DE 19801

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Kunnen, Kevin Lafayette, IN 6 10
Sanchez, Ignacio H Lafayette, IN 3 2

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