Electron-beam melt refining of ferroniobium
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United States of America Patent
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Dec 28, 1999
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N/A
app pub date -
Feb 27, 1998
filing date -
Feb 28, 1997
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Abstract
Niobium, Nb, is refined from FeNb by electron beam melt refining. The amount of the impurities in the FeNb which form suboxides with oxygen is optionally determined. Sufficient oxygen is added to form oxides with these impurities. The electron beam melt refining process is carried out at a sufficiently high temperature and under a sufficiently low vacuum so that the impurities are removed as oxides from the liquid Nb and the purified Nb is recovered. Preferably the oxygen is added as an oxygen-containing compound such as Nb.sub.2 O.sub.5. The recovered Nb can be subjected to additional electron beam melt refining cycles to obtain the desired purity.
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