Synthesis of phase stabilized vanadium and chromium carbides

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United States of America Patent

PATENT NO 5869019
SERIAL NO

08720635

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Abstract

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In order to eliminate the oxygen sensitivity of chromium carbide and vanadium carbide particles, vanadium carbide and chromium carbide particles are formed by carburizing a precursor compound at a elevated reaction temperature of about 950.degree. C. Initially, the precursor compound is heated in an inert nitrogen-containing gas to the reaction temperature. Once the reaction temperature is achieved, hydrogen and a carbon-containing gas such as methane or ethylene are used to conduct the carbonization. After the carbonization has been completed, the carbonizing gas is then replaced with an inert nitrogen-containing gas and the product allowed to cool down. The carbonization cycle is adjusted so that the oxygen level is kept to less than 0.35%, while the nitrogen level is kept at about 2%. Powders produced from this process show minimal or no oxygen pickup when exposed to ambient air.

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Patent Owner(s)

Patent OwnerAddress
N V UNION MINIERE S AGULLEDELLE 92 B-1200 BRUXELLES

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Seegopaul, Purnesh Flemington, NJ 11 111

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