Method of producing the aromatic polyimide

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United States of America Patent

PATENT NO 5821320
SERIAL NO

08856542

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Abstract

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18.4 grams of 4,4'-(hexafluoroisopropyridine)diphthalic acid dianhydride and 7.5 grams of 1,4-phenylenediamine dihydrochloride are mixed in a solvent consisting of 80 ml of N-methyl-2-pyrrolidone and 20 ml of dichlorobenzene and are heated at an argon atmosphere to raise its temperature from a room temperature to 170.degree. C. slowly and to be reacted for five hours while an azeotropic dihydration of water which is generated at 170.degree. C. is conducted. After the reaction is completed, a reaction product is precipitated in methanol, the precipitate is washed with methanol and dried at 80.degree. C. FIG. 1 shows the infrared spectra of the reaction product.

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Patent Owner(s)

Patent OwnerAddress
PETROLEUM ENERGY CENTERA JURIDICAL INCORPORATED FOUNDATION 3-22 AZABUDAI 2-CHOME MINATO-KU TOKYO

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Ikeda, Kenichi Osaka, JP 75 1020
Maeda, Masatoshi Osaka, JP 31 534

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