Chemical process
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United States of America Patent
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Apr 28, 1998
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N/A
app pub date -
Jul 18, 1996
filing date -
Mar 29, 1990
priority date (Note) -
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Abstract
A method of producing 1,1,1,2-tetrafluoroethane in two separation reaction zones involving (1) reaction of trichloroethylene and hydrogen fluoride to produce l,l,l-trifluoro-2-chloroethane and (2) reaction of the 1,1,1-trifluoro-2-chloroethane and hydrogen fluoride to produce 1,1,1,2-tetrafluoroethane wherein both reactions are carried out at superatmospheric pressure, reaction (2) is carried out at a temperature in the range of 250.degree.-450.degree. C., reaction (1) is carried out at a temperature in the range of 200.degree.-400.degree. C. but below that used in reaction (2) and unconverted 1,1,1-trifluoro-2-chloroethane is recycled for further reaction with hydrogen fluoride.
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