Micron-sized nickel metal powder and a process for the preparation thereof

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United States of America Patent

PATENT NO 5584908
SERIAL NO

08340330

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Abstract

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A process is provided for the production of a nickel metal powder by reduction of an ammoniacal nickel (II) carbonate solution essentially free of metallic nickel. A soluble silver salt is added in an amount to provide a soluble silver to nickel weight ratio of 1.0 to 10.0 grams per kilogram of nickel, an organic dispersant, such as gelatin, is added in the amount of 5.0 to 20.0 grams per kilogram of nickel Ni (II), together with a spheroid-promoting agent such as anthraquinone in an amount of about 1.0 to 5.0 grams per kilogram of nickel. The solution is heated to a temperature in the range of 150.degree. to 180.degree. C., with agitation, under a hydrogen pressure of about 3.5 MPa for a time sufficient to reduce the ammoniacal ammonium nickel (II) carbonate solution to micron-sized nickel metal powder. A high purity, micron-sized nickel metal powder of generally spheroid particulate configuration is produced. The nickel metal powder has an average particle size of about 0.5 microns. The metal powder is characterized in having an iron impurity content of less than 100 ppm.

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Patent Owner(s)

Patent OwnerAddress
N V UNION MINIERE S AGULLEDELLE 92 B-1200 BRUXELLES

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Scheie, Hugh C St. Albert, CA 3 24

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