Method for the preparation of carbonated hydroxyapatite compositions
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United States of America Patent
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Nov 28, 1995
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app pub date -
May 18, 1994
filing date -
May 19, 1993
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Abstract
A method for the preparation of a carbonated hydroxyapatite composition which has a density of at least 95% of the theoretical density, which method comprises sintering at substantially atmosphere pressure a green carbonated hydroxyapatite composition containing up to 20% by weight of CO.sub.3.sup.2- ions and having a green density of from 25 to 60% of the theoretical density at a temperature in the range of from 750.degree. to 1450.degree. C. in carbon dioxide containing from 0.001 to 0.10 grams of water per liter of gas, the sintering temperature being selected within the above range and the green composition being sintered for a period of time sufficient to cause the green composition to densify to at least 95% of the theoretical density.
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