Preparation of high cis-1,4-polybutadiene with reduced gel
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United States of America Patent
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May 2, 1995
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N/A
app pub date -
Sep 16, 1994
filing date -
Sep 16, 1994
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Abstract
There is provided a process for the preparation of a high cis-1,4-polybutadiene with a reduced microgel content wherein a novel catalyst system consisting of (1) a nickel salt of a carboxylic acid, (2) a mixture of triethyl aluminum and an organoaluminum compound having the formula R.sub.3 Al, said mixture having an average composition Et.sub.3-x R.sub.x Al wherein Et is an ethyl group, x is a numeral from 0.1 to 2.9 and R is an alkyl group having 8 to 12 carbon atoms, and (3) a boron trifluoride etherate is used to polymerize 1,3-butadiene in an inert hydrocarbon.
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