Carbonylation of allylic alcohols and synthesis of an ambergris fragance compound

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United States of America Patent

PATENT NO 5326888
SERIAL NO

07594249

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A process for the carbonylation of allylic alcohols such as nerolidol, farnesol, or their monocyclic analogues with carbon monoxide at a pressure of at least 30 bar in the presence of a polar solvent and a palladium halide catalyst, optionally an alkali metal halide salt, and optionally an alcoholic solvent. The carbonylated product may then be reduced to the corresponding alcohol, which is cyclized in the presence of Lewis or Bronsted acids to afford an ambergris fragrance compound.

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Patent Owner(s)

Patent OwnerAddress
HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN (HENKEL KGAA)TFP/PATENTABTEILUNG DUESSELDORF D-401

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Cassel, Jonathan M Healdsburg, CA 14 177
Hoagland, Steven M San Fransisco, CA 4 10
Renga, James M Santa Rosa, CA 116 897

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  • 6 Citation Count
  • C07D Class
  • 19.63 % this patent is cited more than
  • 31 Age
Citation count rangeNumber of patents cited in rangeNumber of patents cited in various citation count ranges42314341826720745622301 - 1011 - 2021 - 3031 - 4041 - 5051 - 6061 - 7071 - 8081 - 9091 - 100100 +01002003004005006007008009001000110012001300140015001600

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