Process for producing phosphorous acid

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United States of America Patent

PATENT NO 5085846
SERIAL NO

07685460

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Abstract

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Phosphorous acid is made by a continuous recycling process from a mixture of phosphorous and hydrochloric acids, comprising: (i) continuously recycling the mixture in a loop apparatus; (ii) adding water to and passing phosphorus trichloride into said recycling mixture so as to generate a condition of turbulent flow at the point of contact of the phosphorus trichloride and the recycling mixture, whereby a reaction product, comprising an aqueous solution of phosphorous and hydrochloric acids as a continuous liquid phase and gaseous hydrogen chloride as gas bubbles of disperse phase, is produced; (iii) separating said gaseous hydrogen chloride; (iv) cooling said reaction product; and (v) recycling at least a portion of said reaction product and repeating steps (ii), (iii) and (iv) thereon to produce a more highly concentrated solution of phosphorus acid.

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Patent Owner(s)

Patent OwnerAddress
ALBRIGHT & WILSON LIMITEDWARLEY

International Classification(s)

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Holmes, William S Wolverhampton, GB2 5 68
Lowe, Edward J Stourbridge, GB2 6 37

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