Process of producing phosphate coatings on metals
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United States of America Patent
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Apr 25, 1989
Grant Date -
N/A
app pub date -
Oct 20, 1987
filing date -
Oct 25, 1986
priority date (Note) -
Expired
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Abstract
Disclosed is a process of producing a phosphate coating on a metal having a surface which consists at least in part of iron or steel. The metal is contacted at a temperature in the range from 30.degree. to 50.degree. C. with a phosphatizing solution which contains 5 to 25 g/l zinc, 1 to 10 g/l manganese, 0.1 to 13 g/l iron(II), 5 to 40 g/l phosphate (calculated as P.sub.2 O.sub.5), 5 to 50 g/l nitrate, and which also contains 0.5 to 5 g/l fluoroborate (calculated as BF.sub.4), and 0.05 to 3 g/l tartaric acid and/or citric acid. The solution has been adjusted to weight ratios of Zn:P.sub.2 O.sub.5 =(0.5 to 3):1 and of Mn:Zn=(0.04 to 0.5):1 and to a ratio of free acid to total acid of (0.04 to 0.2):1. It is preferred to add nickel, copper and/or calcium to the phosphatizing solution and to adjust it to a content of Fe(II) not in excess of 10 g/l. The process is particularly suitable for preparing metals for cold working.
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