Process for producing zirconium sols and gels, and process for producing zirconia using the same
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United States of America Patent
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Mar 28, 1989
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app pub date -
Nov 10, 1987
filing date -
Dec 25, 1985
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Abstract
A process for producing acidic boratozirconium chloride sols which comprises: reacting a zirconium compound with a boron compound in molar ratios of B/Zr of 0.3-1.2 together with a compound of a metal M other than boron, the metal M being selected from the group consisting of divalent, trivalent, tetravalent and pentavalent metals in molar ratios of M/Zr of about 0.01-1 in water in the presence of chloride ions in molar ratios of Cl/Zr of not less than about 1. The acidic boratozirconium chloride sol may be converted to basic boratozirconium sols by reacting the acidic sol with a basic carbonate compound such as ammonium carbonate. The sols, either acidic or basic, are readily gelled by contact with a dehydration solvent such as methanol or acetone. The gel is calcined at relatively low temperatures to provide zirconia which is either very pure or stabilized in varied degrees.
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