Dense molded bodies of polycrystalline aluminum nitride and process for preparation without use of sintering aids

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United States of America Patent

PATENT NO 4803183
SERIAL NO

07017776

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Abstract

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The invention is a molded body of polycrystalline aluminum nitride having a density of at least 99.8% TD and comprising: at least 99% by weight AlN up to 0.35% by weight residual oxygen up to 0.35% by weight residual carbon and up to 0.03% by weight metallic impurities (Fe, Si, Ca, Mg). In the molded body, the aluminum nitride is present in the form of a single phase, homogeneous, isotropic microstructure having a maximum grain size of 5 .mu.m. The residual oxygen and the residual carbon are present in the form of a solid solution in the aluminum nitride lattice and caromografically not detectable as separate phase(s) up to a magnification of 2400 times. The molded bodies have a bending strength measured according to the 4-point method, at room temperature and up to about 1400.degree. C., of at least 500 N/mm.sup.2, a predominantly transcrystalline rupture modulus and a thermal conductivity at 300 K of at least 150 W/mK. The molded body is produced from a porous, deoxidized green body having a maximum density of 70% TD and the same chemical composition as the final product, by isostatic hot pressing in a vacuum sealed casing at a temperature of from 1700.degree. to 2100.degree. C. and a pressure of from 100 to 400 MPa in a high-pressure zone using an inert gas as a pressure transmitting agent.

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Patent Owner(s)

Patent OwnerAddress
ELEKTROSCHMELZWERK KEMPTEN GMBH MUNICH WESTDE

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Grellner, Wolfgang Kempten, DE 2 52
Hunold, Klaus Lauben, DE 14 250
Lipp, Alfred Bad Worishofen, DE 21 304
Mohr, Max Kempten, DE 2 52
Schwetz, Karl-Alexander Sulzberg, DE 7 193

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