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Abstract

A process and an apparatus for producing a dysprosium-iron alloy or a neodymium-dysprosium-iron alloy by electrolytic reduction of dysprosium fluoride or neodymium fluoride and dysprosium fluoride in a bath of molten electrolyte, consisting essentially of 20-95% by weight of dysprosium fluoride or a mixture of neodymium fluoride and dysprosium fluoride, 5-80% by weight of lithium fluoride, up to 40% by weight or barium fluoride and up to 20% by weight of calcium fluoride, conducted between one or more iron cathode and one or more carbon anode. The apparatus comprises an electrowinning cell of refractory materials coated inside with a lining resistive to the bath, the carbon anode of constant transverse cross-sectional shape over its length, immersed in the electrolyte bath at its free end, the iron cathode of constant transverse cross-sectional shape over its length, immersed in the electrolyte bath at its free end, a receiver placed on the bottom of the cell for collecting the produced dysprosium-iron alloy or neodymium-dysposium-iron alloy in a liquid state on the tip of the iron cathode, siphoning means for withdrawing the molten alloy pooled in the receiver out of the cell, and feeding means for feeding the iron cathode into the electrolyte bath so as to apply the direct current to the iron cathode with a predetermined current density.

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