Process for the production of crystalline silicate ISI-4 using ethylene glycol

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United States of America Patent

PATENT NO 4657750
SERIAL NO

06713086

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Abstract

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Crystalline silicates and processes for the production thereof are described. These crystalline silicates are of new crystalline structure, which, as determined after calcination in the air at 550.degree. C., have a composition represented by the general formula (I): pM.sub.2/n O.Al.sub.2 O.sub.3.qSiO.sub.2 (the symbols are as defined in the appended claims) and give a X-ray diffraction pattern as shown in Table 2. They are superior in heat resistance and acid resistance, and can be used as catalysts for the conversion of various organic compounds, absorbents, or as catalysts for various reactions. They are produced by reacting an aqueous mixture comprising (a) a silica source, (b) an alumina source, (c) an alkali metal and/or alkaline earth metal source, and (d) ethylene glycol or (e) monoethanolamine at a temperature of 100.degree. to 300.degree. C. till the desired crystalline silicates are formed. Although ethylene glycol and monoethanolamine do not remain in the crystalline silicates, they play important roles in the formation of the desired crystalline structure in the course of the production thereof.

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Patent Owner(s)

Patent OwnerAddress
RESEARCH ASSOCIATION FOR PETROLEUM ALTERNATIVES DEVELOPMENTCHIYODA-KU TOKYO

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Kawata, Noboru Ichihara, JP 2 21
Takatsu, Kozo Sodegaura, JP 17 125

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