Process for preparing silica base for dentifrice
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United States of America Patent
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Apr 8, 1986
Grant Date -
N/A
app pub date -
Oct 17, 1984
filing date -
Mar 8, 1983
priority date (Note) -
Expired
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Abstract
Silica base material for dentifrice having excellent transparency, prolonged stability and desired abrasiveness, has specific surface areas measured by BET method and CTAB method of 5-60 m.sup.2 /g respectively with a difference therebetween of less than 40 m.sup.2 /g, and having a refractive index of 142-1.45. This base material can be prepared by reacting an alkali metal silicate solution with hydrochloric acid or sulfuric acid in the presence of an electrolyte in two stages, a silica crystallization stage in which the pH of the reaction system is brought to 10.0, and a neutralization stage in which the pH of the reaction system is brought to 8.0-6.5, completing the neutralization stage within 30 minutes and aging the neutralized mixture for at least 10 minutes. The ratio of the rate of addition of chloride or sulfate ions between the neutralization and crystallization stages is at least 5:3.
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