Process for the preparation of aliphatic azo compounds using an amine coupling

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United States of America Patent

PATENT NO 4546174
SERIAL NO

06578130

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ATTORNEY / AGENT: (SPONSORED)

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Abstract

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There is described a process for the production of a compound of formula I, ##STR1## in which at least one each of R.sub.1, R.sub.2 and R.sub.3, and of R.sub.4, R.sub.5 and R.sub.6, represents an electron withdrawing group, or one of R.sub.1, R.sub.2 and R.sub.3 together with one of R.sub.4, R.sub.5 and R.sub.6 form a --CO-- group, and the remainder of R.sub.1, R.sub.2, R.sub.3, R.sub.4, R.sub.5 and R.sub.6, which may be the same or different, each represent an electron withdrawing group, alkyl, cycloalkyl, phenyl or phenylalkyl, or R.sub.1 and R.sub.2, or R.sub.4 and R.sub.5 , and R.sub.1 and R.sub.4, may together form a --(CH.sub.2).sub.n --chain, in which n is a whole number up to 5, the alkyl, cycloalkyl, phenyl or phenylalkyl group or the --(CH.sub.2).sub.n --chain optionally being substituted, which comprises reacting a compound of formula II, ##STR2## in which R.sub.1 a, R.sub.2 a and R.sub.3 a have the same significances as R.sub.1, R.sub.2, and R.sub.3 above, and some additional significances, with a compound of formula III, ##STR3## in which R.sub.4 a, R.sub.5 a and R.sub.6 a have the same significances as R.sub.4, R.sub.5 and R.sub.6 above, and some additional significances, the reaction being carried out in an aqueous medium in the presence of a base and a surfactant.

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Patent Owner(s)

Patent OwnerAddress
SCHERING INDUSTRIAL PRODUCTS LIMITEDCAMBRIDGE CB3 ODA

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Pollard, Michael D Cambridge, GB2 1 0
Smythe, Stephen R Cambridge, GB2 2 0
Whitmore, Martyn W Cambridge, GB2 1 0

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