PROCESS OF MAKING ABALOPARATIDE
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United States of America Patent
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Issued Date -
Jun 13, 2024
app pub date -
Sep 25, 2023
filing date -
May 20, 2022
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Disclosed herein is an improved process for preparing abaloparatide. The process generally utilizes solid phase peptide synthesis employing an Fmoc-protection scheme. Incorporating a systematic recoupling step of a glutamine residue (Gln16) has been found to minimize the formation of an undesirable des-Gln16 abaloparatide impurity, which is often obtained in significant quantities in the conventional process.
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