PRODUCTION OF MoO2Cl2
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United States of America Patent
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Issued Date -
Mar 14, 2024
app pub date -
Dec 2, 2021
filing date -
Dec 23, 2020
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Abstract
The invention relates to a method for producing MoO2Cl2 under inert conditions, comprising the steps of:
- (i) charging a reaction vessel with MoO2,(ii) reacting the MoO2 with supplied Cl2 in the reaction vessel at a first temperature T1 to give gaseous MoO2Cl2,(iii) transferring the gaseous MoO2Cl2 into a receiving vessel,(iv) resublimating the gaseous MoO2Cl2 in the receiving vessel to give solid MoO2Cl2 at a second temperature T2 that is lower than T1, and(v) recovering solid MoO2Cl2 with a purity determined by ICP-OES/MS of 99.9996 wt. % or more.
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