FLOW SYNTHESIS OF RDX
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United States of America Patent
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Feb 15, 2024
app pub date -
Dec 1, 2021
filing date -
Dec 9, 2020
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Abstract
The invention relates to a method for the flow synthesis manufacture of RDX, comprising the steps of preparing input flow reagent A, comprising hexamine dissolved in nitric acid with a concentration less than 92%, preparing input flow reagent B comprising 99% concentration nitric acid, causing the input flow reagents A and B to enter a flow reactor at a flow rate, so as to cause a total nitric acid concentration of greater than 93%, in said flow reactor, cooling the reaction chamber to less than 30° C., causing the output mixed flow to be quenched.
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