METHOD FOR PRODUCING HOLLOW PARTICLES AND HOLLOW PARTICLES
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United States of America Patent
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Nov 30, 2023
app pub date -
Oct 26, 2021
filing date -
Oct 30, 2020
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Abstract
A method for producing hollow particles which have a void ratio of 50% or more, the method comprising: preparing a mixture liquid containing a polymerizable monomer, a hydrophobic solvent, an aqueous medium, etc., suspending the mixture liquid to prepare a suspension in which droplets of a monomer composition containing the polymerizable monomer, the hydrophobic solvent, etc., are dispersed in the aqueous medium, and subjecting the suspension to a polymerization reaction to prepare a precursor composition containing precursor particles having a hollow portion surrounded by a shell and filled with the hydrophobic solvent, wherein the polymerizable monomer a hydrocarbon monomer, and in 100% by mass of the polymerizable monomer, a content of a crosslinkable monomer containing two or more ethylenically unsaturated double bonds is 70% by mass or more, and wherein the hydrophobic solvent is a hydrocarbon solvent containing 5 to 8 carbon atoms.
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