Method for Analyzing Content and Distribution of Boron Introduced Into Positive Electrode Active Material
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United States of America Patent
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Oct 12, 2023
app pub date -
Sep 1, 2021
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Dec 22, 2020
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Abstract
A method for analyzing the content of boron in a cathode active material is disclosed herein. In some embodiments, a method comprises (S1) introducing boron into a cathode active material to prepare a cathode active material sample, (S2) separating a first liquid layer and a first precipitate by dissolving the sample in water, treating the first liquid layer with acid to form a first resulting solution, and measuring the boron concentration in the first resulting solution by inductively coupled plasma optical emission spectroscopy (ICP-OES), (S3) separating a second liquid layer and a second precipitate by dissolving the first precipitate in water, treating the second liquid layer with acid to form a second resulting solution, and measuring the boron concentration of the second resulting solution by ICP-OES, and (S4) measuring the boron concentration of a third resulting solution, obtained by adding acid and hydrogen peroxide to the second precipitate, by ICP-OES.
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